DMF.

The obtaining of nanostructured gold in dimethylformamide solutions of HAuCl4 has been investigated. The morphology of gold deposited by chronoamperometry and pulse regime of deposition on the glassy carbon surface was studied. It is established, with growth of cathodic potential values at constant electrical mass the quantity of gold particles is increased and a tendency to agglomeration at stationary electrolysis is observed. Pulse electrodeposition mode allows to obtaining gold nanoparticles with relatively the same geometry and a uniform distribution over the surface.