For the first time synthesized and studied complexes of nitrosopentacyanide of iron (II) with complex cations of d-metals. The processes of thermal transformation of nitrosopentacyanide of iron (II) with complex cations of d-metals have been studied. The influence on the course of thermal transformations of the nature of the d-metal and the composition of the gas phase is shown. It was established that the thermal stability and character of the thermolysis of complex binuclear complexes depend on the method of coordination and the mutual placement of ligands in the coordination sphere.
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