Аналітичний контроль процесів одержання алкілциклогексенкарбоксилатів методом газорідинної хроматографії
The optimum conditions for the method of isothermal gas-liquid chromatography for the reaction mixtures analysis of acrylic acid ester derivatives to 2,3 dimethylbut-1,3-diene cycloaddition are determined. The evaluation of the chromatographic system efficiency and the resolution options has been provided. Chromatographic retention of cycloaddition products in relation to their structure was considered. The main metrological characteristics of the quantitative chromatographic analysis by internal normalization method are calculated.