synthesis

Model Development and Structural-Parametric Synthesis of a Fractional- Order Speed Controller of theFC-AM System

In modern industry, the most widely used are adjustable electric drives of the ‘Frequency converter - induction motor’ (FC-AM) system, in which integer-order controllers are mainly implemented and used. The use of fractional-order controllers in electromechanical FC-AM systems allows to ensure: higher quality of transition processes, increase the stability margin and reliability of the system, higher robustness to changes in motor parameters and, as a result, guarantees higher performance compared to classical integer controllers.

OLEOCHEMICAL COMPOUNDS AS MULTIFUNCTIONAL INGREDIENTS OF DRY BUILDING MIXTURES

 Alkaline salts of maleated diethanolamides of fatty acids of vegetable oils have been synthesized - effective multifunctional additives that improve the technological and operational properties of dry building mixtures. A key advantage of the synthesized compounds is the use of accessible and renewable raw materials. The most pronounced overall effect was observed for the potassium and, especially, the lithium SMDFA, indicating the need for further in-depth studies.  

Synthesis of Multi-Bit Pyramidal Adders on FPGA

The paper analyses the system characteristics and functional capabilities of multi-bit pyramidal adders that can be used in the structures of discrete perceptron of modern neural networks for summing weight coefficients and input signals. The methodology for designing multi-bit adders using flow and spatial-temporal graphs is described. Algorithmic and recursive pyramidal adders have been developed and their main system characteristics have been determined.

Synthesis and Thermodynamic Parameters of Phase Transitions of 3-(1-R-5-Phenyl-1H-Pyrrol-2-yl)propanoic Acid Derivatives

A series of 3-(1-R-5-phenyl-1H-pyrrol-2-yl)propanoic acids (R = H, Ar, Alk, Hetaryl) was obtained via the reaction of 4,7-dioxo-7-phenylheptanoic acid with amines. The enthalpies of vaporization and fusion of eight compounds were experimentally determined using differential thermal and thermogravimetric methods of analysis for the first time.

Research and design of a matrix multiplier on FPGA

This paper presents a comprehensive investi- gation and hardware implementation of a multi-bit Brawn matrix multiplier architecture. The research focuses on analyzing the system characteristics of binary multipliers realized with both conventional and optimized full and half adders. Particular attention has been given to the applicability of such multipliers within arithmetic logic units (ALUs) for vector and scalar processing architectures. Analytical models have been formulated to quantify hardware resource utilization and computational latency across various logic base configurations.

Synthesis, Structure and Electrophysical Properties of Fluoride-Conducting Phases Вa1-XLaXSnF4+X

It has been determined that the concentration interval for the existence of solid solutions of heterovalent substitution $\mathrm{Ba}_{1-\mathrm{x}} \mathrm{La}_{\mathrm{x}} \mathrm{SnF}_{4+\mathrm{x}}$, which are formed by the partial replacement of barium cations with lanthanum cations in the $\mathrm{BaSnF}_4$ compound, is $0.0<x \leq 0.12$. The obtained phases are isostructural $\mathrm{BaSnF}_4$, have a crystal lattice of tetragonal syngony, corresponding to the $\mathrm{P} 4 / \mathrm{nmm}$ space group.

Synthesis of PI- and PID-Regulators in Control Systems Derived by the Feedback Linearization Method

The work proposes a comprehensive approach to the synthesis of the coefficients of PI- and PID-controllers, as well as the coefficients of feedback based on the state variables of the system, using the feedback linearization method for the synthesis of control influences. This approach considers not only the static but also the dynamic characteristics of the system, allowing for higher control accuracy. The feedback linearization method facilitates the transformation of nonlinear systems into linear ones, simplifying their further analysis and controller design.

Synthesis of Some Azo Dyes Based on 2,3,3-Trimethyl-3H-indolenine

New azo compounds on the base of 2,3,3-trimethyl-3H-indolenine were synthesized and characterized by FT-IR, NMR, and Mas-spectral analysis. The synthesis was conducted in three different pathways: 1) by reducing the nitro compound with Zn/NaOH in alcohol; 2) by heating of 2,3,3-trimethyl-3H-indolenine-5-amine in the presence of MnO2 in toluene, and 3) by diazotization of 2,3,3-trimethyl-3H-indolenine-5-amine and treating the resulting diazonium salt with the appropriate coupler.

Synthesis of Heterocyclic Pyridine-Based Chalcones with Dimeric Structure

Three new heterocyclic chalcones containing pyridine moiety were synthesized and their chemical structures were determined via IR, 1H NMR and 13C NMR spectroscopy. General name of these compounds are α,ω-bis{3-(pyridin-3-yl)-1-(phenyl-4-oxy)prop-2-en-1-one}alkanes. The chalcones are dimers having a symmetrical structure and they can be differed by the alkyl spacer length (CnH2n, where n = 8, 10 or 12). Differential scanning calorimetry (DSC) technique was employed to study their phase transition behaviors.

Electrosynthesis of Ni-Co/Hydroxyapatite as a Catalyst for Hydrogen Generation via the Hydrolysis of Aqueous Sodium Borohydride (NaBH4) Solutions

To generate hydrogen from its storage as NaBH4, a catalyst was synthesized via an electrochemical method. The catalyst, Ni-Co, had hydroxyapatite as a support catalyst. The electrochemical cell consisted of a DC power supply, a carbon anode and cathode, and a bipolar membrane to separate the cell into two chambers. The current density was adjusted to 61, 91, and 132 mA/cm2. The electrolysis time was 30, 60, and 90 min. The particles produced were analyzed by XRD and SEM/EDX and tested in the hydrolysis of NaBH4 for hydrogen generation.