The thermochemical fuel properties of melon seed husk (MSH) were characterized to examine its solid biofuel (SBF) potential for future bioenergy utilization. MSH is a cheap, abundant and renewable source of lignocellulosic waste generated from the extraction of vegetable oil from melon seeds. Thermochemical characterization was examined by proximate, ultimate, and thermogravimetric (TG-DTG) analyses, as well as Fourier transform infra-red (FT-IR) spectroscopy. The results showed that MSH exhibits significant volatile matter, fixed carbon, carbon and low nitrogen, sulphur and ash content with a heating value (HHV) of 19.02 MJ/kg. FT-IR analysis indicated functional groups for aliphatic, ester, ketone, alcohol, and aromatic compounds. Thermal decomposition of MSH occurred in three stages: drying (303–448 K), devolatization (448–673 K) and char degradation (673–1073 K).
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