thermal analysis

Розроблення дискретної моделі знаходження ефективних теплофізичних характеристик композитних матеріалів

Описано спосіб розрахунку теплофізичних характеристик композитних матеріалів зі складною внутрішньою структурою на основі дискретної моделі, що будується за методом теплоелектричних аналогій.

This paper consider the method of calculation the thermophysical characteristics of composite materials with complex internal structure based on the discrete model that is constructed by the method of thermal-electric analogies.

Study of the influence of regime factors on the kinetics of the dehydration process of iron (ii) sulfate heptahydrate using the filtration method

The filtration method of gradual dehydration of Iron(II) sulfate heptahydrate hase been proposed. Based on the generalization of experimental data of hydrodynamics, the calculated dependence Euзовн=155∙Reзовн-0,55∙Hdч  was obtained, which makes it possible to determine theoreticallypressure losses in the stationary layer of FeSO4·7H2O.According to the results of complex thermal analysis, the regularities of the gradual dehydration process of FeSO4·7H2O have been established in different temperature intervals.

Use of Activated Clinoptilolite for Direct Dye-Contained Wastewater Treatment

This work reveals a method of complex thermal and chemical activation of natural clinoptilolite from Sokyrnytsky deposit. The chemical activation of a mineral was carried out by HCl solutions treatment at various ratios of liquid-to-solid phases. With the use of thermal and infrared (IR) spectroscopic analyses, the adsorption property of a natural and activated clinoptilolite has been examined for water vapor. The ability of complexly activated clinoptilolite to adsorb direct dyes from their aqua solutions has been investigated.

Biosynthesis Products of Pseudomonas sp. PS-17 Strain Metabolites. 1. Obtaining and Thermal Characteristics

Biogenic surfactants (rhamnolipid biocomplex, dirhamnolipid and exopolysaccharide) and polyhydroxyalkanoate biopolymer which are the new biosynthesis products of Pseudomonas sp. PS-17 strain have been obtained. The thermal transformation of these products has been studied in the air in the temperature range of 293–1273 K. Thermolysis and IR spectroscopy revealed a formation of rhamnolipid biocomplex between rhamnolipids and exopolysaccharide upon acidification of the culture fluid supernatant to pH = 3. Cellular polymer – polyhydroxyalkanoate – was identified by UV-Vis spectroscopy.

Synthesis and properties of niobium-containing silicate glass

The chemical compositions and properties of glass of different systems for the production of glass ionomer dental cements (GIC) were analyzed. For the synthesis of glass, the basic system 4SiO2–3Al2O3 – xNb2O5 – CaO with the content of Nb2O5 8.8 and 16.2% (wt.) is proposed. High-temperature technology and parameters of glass production for GIC are presented in the article. The properties of synthesized niobium-containing glass were determined and analyzed. The effect of niobium oxide on the crystallization ability of glass was determined by the method of differential thermal analysis.

Рhysical and chemical researches on the structure of humic acids

Based on the complex thermal, titrimetric and UV/Vis spectral analyzes, the structure and the content of functional groups in the molecules of humic acids obtained from different raw materials – coprolite, peat and leonardite – were investigated. The thermal stability of the substances was investigated in the air in the temperature range 20-1000°C. It has been found that the content of the aliphatic component is predominant in humic acids obtained from different raw materials.

Finding effective thermal characteristics of composite materials based on the analysis of thermal conductivities

This paper presents a method and algorithm for finding effective thermal characteristics of composite materials, with complex internal structure by the method of thermal-electrical analogies based on the discrete model that built for the task of analysis of the temperature field by finite element method.